Skip to main content
ELECTRICAL MEASURING INSTRUMENTS For the detection or measurement of electric current, potential difference, and resistance certain instruments have been devised viz. The galvanometer for the detection of small currents measurements of small currents of the order of micro amperes or mili amperes the voltmeter or potentiometer for the measurement of potential difference (and voltage) between two points of a circuit are the EMF of a source the ammeter for the measurement of large currents the wheatstone bridge the meter Bridge the post office box and the ohmmeter for the measurement of resistance. THE MOVING COIL GALVANOMETER The moving coil galvanometer is a basic electrical instrument it is used for the detection (and Measurement) of small currents. Its underlying principle is the fact that when a current flows in a rectangular coil placed in a magnetic field it experiences a magnetic torque. If it is free to rotate under a controlling torque, it rotates through an angle proportional t...

HOW TO PREPARE POTASH ALUM?

OBJECT :

To prepare potash alum (K2SO4,Al2(SO4)3.24H2O)

APPARATUS :

China dish,beaker,watch glass,funnel,conical flask,glass rod,filter paper,water trough,wire gauze,tripod stand and bunsen burner.

CHEMICALS :

Solid Aluminium sulphate [Al2(SO4)3.16H2O](7.7 gms) , K2SO4 (2.0 gms), 50 mls of distilled water,few drops of conc H2SO4

EQUATIONS :

K2SO4 +Al2 (SO4)3.16H2O + 8H2O --------------> K2SO4.Al2(SO4)3.24H2O

THEORY :

The term alum was originally used for potassium aluminium sulphate [K2SO4.Al2(SO4)3.24H2O] commonly known as potash alum.The term alum is now used for all double sulphates having general formula R2SO4.M2(SO4)3.24H2O

PROCEDURE :

Weigh out 7.7 gm of aluminium sulphate and dissolve it in about 30 mls of boiling distilled water.Add few drops of H2SO4 (conc) to make the solution clear.In another beaker dissolve 2.0 g of K2SO4 in 20 mls of distilled water.Mix the two solutions and concentrate the solution to crystallization by heating it in a china dish.Now cool this concentrated solution in ice cold water.After few minutes, crystals of alum separates out.

RESULT :

Colorless crystals of potash alum are obtained.

Comments

Popular posts from this blog

NUCLEAR RADIATIONS INTERACTION OF NUCLEAR RADIATIONS WITH MATTER In the previous article we have discussed natural radioactivity in which  α and β particles and γ-rays are emitted from the disintegrating nucleus of an atom.In nuclear fission and fusion reactions neutrons and other particles together with certain radiations are emitted from the nucleus.Moreover, interaction of high energy particles (neutral or artificial) with matter produce certain nuclear or atomic reactions with emission of particles like protons,deutrons,neutrons and ionizing radiations like γ-rays from the nucleus and x-rays and ultraviolet rays from the atom.These particles and radiations have been studied carefully for their properties and effects with are as follows: ALPHA (α)  PARTICLES It shoots out from the nucleus with a high velocity ( 0.1 × 10 ^ 8 m/s ). Thus it possesses very high energy 7.7 MeV for the most energetic from R ac.Due to its large size more charge and high energy it can make very l...
Periodic Classification of Elements :   "The arrangement of elements in their blocks,periodic and groups is called classification of elements. Dobereiner's Classification :   In 1829, W. Dobereiner, a German Chemist,made use of Idea of relationship between atomic masses and properties of elements for the classification of elements.He arranged similar elements in to groups of three elements call "triads". Law of Triads : "The atomic mass of the middle element was found to be approximately the average of the other two elements of triads". This is know as "Law of Triads" Li = 7 Na + 23+39/2 =23 K = 39 This classification could not be extended to all elements for their classification. New Land's Classification : In 1864.New Land  an English chemist attempted the classification of elements in order of their increasing atomic masses.He observed the properties of elements & found that properties of elements. Law of Octave : "The properties...
THE ATOMIC NUCLEUS INTRODUCTION: The beginning of twentieth century. not only witnessed the successful development of atomic hypothesis the old quantum theory of radiation by plank, and Einsteins special theory of relativity; these years also marked the beginning of nuclear physics as a new field of scientific activity. In 1886 Henri Bacqueral first observed the phenomena of radioactivity.A year after J.J Thomson discovered the electron.Later on Thomson demonstrated that cathode rays were constituted of electrons..In the way of notion of the atom as the ultimate indivisible unit of matter had to be discarded, and it become evident that atoms included electrons among their structure and these electrons could be liberated by electromagnetic excitation as in a gas discharge spontaneously as in radio activity. In 1902 Rutherford and Soddy showed that in radioactive decay an atom transform itself into a different chemical element.This discovery led to the development of models for nuclear s...